((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde

Base Information

Chemical Name:((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde
CAS No.:97855-72-6
Molecular Formula:C₁₄H₂₄O₃
Molecular Weight:240.343
Hs Code.:

Synonyms:

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Chemical Property of ((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde

Chemical Property:

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Technology Process of ((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde

There total 13 articles about ((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 97855-71-5
(+)-(1S,2S)-2-allyl-1,3,3-trimethylcyclohexanecarbaldehyde ethylene acetal

: 97855-72-6
((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde

Guidance literature:: With sodium periodate; osmium(VIII) oxide;
DOI:10.1016/S0040-4039(00)98546-0

Reference yield:

: 110715-80-5
(-)-(1S,8aS)-1,2,3,5,6,7,8,8a-octahydro-5,5,8a-trimethylnaphthalen-1-ol

: 97855-72-6
((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde

Guidance literature:: Multi-step reaction with 12 steps

1: 95 percent / H₂ / Adam's catalyst / acetic acid

2: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

4: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

5: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

6: NaBH₄ / methanol / 0.33 h / Ambient temperature

7: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

8: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

9: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

10: 88 percent / Florisil, PCC / CH₂Cl₂ / 1 h / Ambient temperature

11: 98 percent / toluene-p-sulphonic acid / benzene / 0.33 h / Heating

12: 1. osmium tetraoxide; 2.) sodium periodate / 1.) diethyl ether, water, rt, 5 min; 2.) rt, 10 h.

With lead(IV) acetate; sodium hydroxide; sodium tetrahydroborate; florisil; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; pyridinium chlorochromate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 110654-75-6
(+)-(4aS,5S)-5-benzoyloxy-3,4,4a,5,6,7-hexahydro-1,1,4a-trimethylnaphthalen-2(1H)-one

: 97855-72-6
((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-acetaldehyde

Guidance literature:: Multi-step reaction with 13 steps

1: 93 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 6 h / Heating

2: 95 percent / H₂ / Adam's catalyst / acetic acid

3: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

4: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

5: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

6: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

7: NaBH₄ / methanol / 0.33 h / Ambient temperature

8: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

9: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

10: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

11: 88 percent / Florisil, PCC / CH₂Cl₂ / 1 h / Ambient temperature

12: 98 percent / toluene-p-sulphonic acid / benzene / 0.33 h / Heating

13: 1. osmium tetraoxide; 2.) sodium periodate / 1.) diethyl ether, water, rt, 5 min; 2.) rt, 10 h.

With lead(IV) acetate; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; florisil; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; hydrazine hydrate; pyridinium chlorochromate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; diethylene glycol; benzene;