Technology Process of 2-(3,5-dimethylphenyl)-5,7-diisobutylquinoline
There total 3 articles about 2-(3,5-dimethylphenyl)-5,7-diisobutylquinoline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0);
In
water; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tris(triphenylphosphine)ruthenium(II) chloride; potassium hydroxide / toluene / 18 h / Reflux; Dean-Stark
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate monohydrate / toluene; water / Inert atmosphere; Reflux
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); tris(triphenylphosphine)ruthenium(II) chloride; potassium phosphate monohydrate; potassium hydroxide;
In
water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Cooling with ice
2: tris(triphenylphosphine)ruthenium(II) chloride; potassium hydroxide / toluene / 18 h / Reflux; Dean-Stark
3: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate monohydrate / toluene; water / Inert atmosphere; Reflux
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); lithium aluminium tetrahydride; tris(triphenylphosphine)ruthenium(II) chloride; potassium phosphate monohydrate; potassium hydroxide;
In
tetrahydrofuran; water; toluene;
