[chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

Base Information

Chemical Name:[chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]
CAS No.:537035-75-9
Molecular Formula:C₁₇H₂₉ClN₆P₂Ru
Molecular Weight:515.928
Hs Code.:

Synonyms:[chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

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Chemical Property of [chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

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Technology Process of [chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

There total 1 articles about [chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 53597-69-6
(1,3,5-triaza-7-phosphaadamantane)

: 537035-75-9
[chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

: 877864-62-5
[(η⁵-cyclopentadienyl)Ru(1,3,5-triaza-7-phosphaadamantane)(PPh₃)Cl]

Guidance literature:: In toluene; (N2); reflux;
DOI:10.1021/om060892x

Reference yield: 78.0%

: 537035-75-9
[chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

: 311801-17-9
8-benzylthiotheophylline

: 1263431-31-7
[(C5H5)Ru(1,3,5-triaza-7-phosphaadamantane)2(8-benzylthio-theophyllinate-κS)]

Guidance literature:: With KOH; In water; (N2); std. Schlenk technique; ligand was dissolved in aq. KOH; stirred for 15 min; Ru complex was added; refluxed for 4 h; concd. (vac.); filtered; washed (EtOH, Et2O); dried (vac.); elem. anal.;
DOI:10.1021/ic101466u

Reference yield: 57.0%

: 5952-62-5
sodium 4-(diphenylphosphino)benzenesulfonate

: 537035-75-9
[chlorobis(1,3,5-triaza-7-phosphaadamantane-P)(cyclopentadienyl)ruthenium(II)]

: cyclopentadienidoruthenium(II)I(PPh₂(3-OSO₂C₆H₄))(1,3,5-triaza-7-phosphaadamantane)2

Guidance literature:: In methanol; byproducts: NaCl; (N2), Ru complex in CH3OH added to solid ligand (1 equiv.), refluxed for5 h; filtered hot, eashed (CH3OH, Et2O), dried (vac.), elem. anal.,;
DOI:10.1002/ejic.200601177