Technology Process of C31H29FN2O5
There total 5 articles about C31H29FN2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1.1,2,3,4-tetrahydro-1,5-naphthyridine;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
for 0.166667h;
Cooling with ice;
C24H23FO6;
In
tetrahydrofuran; hexane;
for 0.5h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 2 h / 20 °C / Cooling with ice
1.2: 20 °C
2.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 6 h / 50 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / Cooling with ice
3.2: 0.5 h / Cooling with ice
With
n-butyllithium; boron tribromide; potassium carbonate; sodium iodide;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hexamethylenetetramine / 2.5 h / 80 °C
2.1: SULFAMIDE; sodium chlorite / 1,4-dioxane; water / 0.5 h / Cooling with ice
3.1: boron tribromide / dichloromethane / 2 h / 20 °C / Cooling with ice
3.2: 20 °C
4.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 6 h / 50 °C
5.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / Cooling with ice
5.2: 0.5 h / Cooling with ice
With
sodium chlorite; n-butyllithium; hexamethylenetetramine; boron tribromide; potassium carbonate; SULFAMIDE; sodium iodide;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; N,N-dimethyl-formamide;
