tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

Base Information

Chemical Name:tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate
CAS No.:1413935-91-7
Molecular Formula:C₁₈H₂₀O₁₀S₄
Molecular Weight:524.615
Hs Code.:

Synonyms:tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

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Chemical Property of tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

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Technology Process of tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

There total 3 articles about tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 118-75-2
chloranil

: 2365-48-2
Methyl thioglycolate

: 1413935-91-7
tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

Guidance literature:: Methyl thioglycolate; In water; for 0.0833333h; Green chemistry;

chloranil; With potassium carbonate; In water; at 20 ℃; for 3h; regioselective reaction; Green chemistry;
DOI:10.1016/j.ejmech.2012.07.022

Reference yield: 46.0%

: 67-56-1
methanol

: 6285-66-1
(2,4,5-tris-carboxymethylsulfanyl-3,6-dihydroxy-phenylsulfanyl)-acetic acid

: 1413935-91-7
tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

Guidance literature:: With silver nitrate; at 60 ℃; for 6h;
DOI:10.1016/j.poly.2017.08.035

Reference yield:

: 106-51-4
p-benzoquinone

: 1413935-91-7
tetramethyl 2,2',2'',2'''-(3,6-dioxocyclohexa-1,4-diene-1,2,4,5-tetrayl)tetrakis(sulfanediyl)tetraacetate

Guidance literature:: Multi-step reaction with 2 steps

1: water / 0.5 h

2: silver nitrate / 6 h / 60 °C

With silver nitrate; In water;
DOI:10.1016/j.poly.2017.08.035