2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine
CAS No.:1179983-76-6
Molecular Formula:C₂₀H₂₂F₂N₂O
Molecular Weight:344.404
Hs Code.:

Synonyms:2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

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Technology Process of 2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

There total 3 articles about 2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1179983-75-5
2-(4-benzyloxy-5,7-difluoro-1H-indol-3-yl)-N,N-dimethylethanamine

: 74-88-4
methyl iodide

: 1179983-76-6
2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

Guidance literature:: 2-(4-benzyloxy-5,7-difluoro-1H-indol-3-yl)-N,N-dimethylethanamine; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

methyl iodide; In N,N-dimethyl-formamide;

Reference yield:

: 1179983-74-4
2-(4-benzyloxy-5,7-difluoro-1H-indol-3-yl)-N,N-dimethyl-2-oxoacetamide

: 1179983-76-6
2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / 1,4-dioxane / Reflux

2: sodium hydride / N,N-dimethyl-formamide / 0 °C

With lithium aluminium tetrahydride; sodium hydride; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 52061-51-5
4-Benzyloxyindol-3-yl-N,N-dimethylglyoxylamide

: 1179983-76-6
2-(4-(benzyloxy)-5,7-difluoro-1-methyl-1H-indol-3-yl)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: Selectfluor / acetonitrile / 20 °C

2: lithium aluminium tetrahydride / 1,4-dioxane / Reflux

3: sodium hydride / N,N-dimethyl-formamide / 0 °C

With lithium aluminium tetrahydride; sodium hydride; Selectfluor; In 1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;