N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate

Base Information

Chemical Name:N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate
CAS No.:1159373-59-7
Molecular Formula:C₂₃H₃₃BF₃NO₆
Molecular Weight:487.324
Hs Code.:

Synonyms:N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate

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Technology Process of N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate

There total 2 articles about N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1351337-49-9
(CF₃)(H₂N)C₆H₃B(pinacolate)

: 1159373-59-7
N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate

Guidance literature:: With dmap; In tetrahydrofuran; at 25 - 50 ℃;

Reference yield: 76.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1159373-58-6
(CF₃)(O₂N)C₆H₃B(pinacolate)

: 1333-74-0
hydrogen

: 1159373-59-7
N,N'-di-tert-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trifluoromethyl)phenylcarbamate

Guidance literature:: With palladium on activated charcoal; In methanol; treatment of boronic acid deriv. with H2 in methanol in presence of Pd/C, treatment of obtained amine with dicarbonate deriv. in THF in presenceof pyridine deriv.;