5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

Base Information

Chemical Name:5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester
CAS No.:315245-29-5
Molecular Formula:C₂₆H₂₈O₅Si
Molecular Weight:448.591
Hs Code.:

Synonyms:5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

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Chemical Property of 5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

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Technology Process of 5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

There total 4 articles about 5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 67-56-1
methanol

: 269411-88-3
5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid diethyl ester

: 315245-29-5
5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

Guidance literature:: With sodium hydroxide; at 23 ℃; for 72h;
DOI:10.1021/jm9903242

Reference yield: 87.0%

: 269411-88-3
5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid diethyl ester

: 315245-29-5
5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

Guidance literature:: With sodium hydroxide; citric acid; In methanol; at 23 ℃; for 72h;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 315245-29-5
5-(tert-butyl-diphenyl-silanyloxymethyl)-isophthalic acid monomethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 39.9 g / imidazole / dimethylformamide / 23 °C

2: 87 percent / 0.95 N aq. NaOH / 72 h / 23 °C

With 1H-imidazole; sodium hydroxide; In N,N-dimethyl-formamide; 1: silylation / 2: methanolysis;
DOI:10.1021/jm9903242