Technology Process of C26H25N3O3S
There total 5 articles about C26H25N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / dichloromethane / 0.5 h / 0 - 20 °C
2.1: pyridine / isopropyl alcohol / 72 h / 60 °C
3.1: sodium hydroxide / tetrahydrofuran; methanol; water / 3 h / 60 °C
3.2: 3 h
4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
With
pyridine; thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 2.5 h / 20 °C / Reflux
2.1: thionyl chloride / dichloromethane / 0.5 h / 0 - 20 °C
3.1: pyridine / isopropyl alcohol / 72 h / 60 °C
4.1: sodium hydroxide / tetrahydrofuran; methanol; water / 3 h / 60 °C
4.2: 3 h
5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
With
pyridine; thionyl chloride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol; mineral oil;