C₃₇H₄₈Br₂OSi

Base Information

Chemical Name:C₃₇H₄₈Br₂OSi
CAS No.:1526916-02-8
Molecular Formula:C₃₇H₄₈Br₂OSi
Molecular Weight:696.681
Hs Code.:

C<sub>37</sub>H<sub>48</sub>Br<sub>2</sub>OSi

Synonyms:C₃₇H₄₈Br₂OSi

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Chemical Property of C₃₇H₄₈Br₂OSi

Chemical Property:

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Technology Process of C₃₇H₄₈Br₂OSi

There total 6 articles about C₃₇H₄₈Br₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 558-13-4
carbon tetrabromide

: 1526916-01-7
C₃₆H₄₈O₂Si

: 1526916-02-8
C₃₇H₄₈Br₂OSi

Guidance literature:: carbon tetrabromide; With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.166667h;

C₃₆H₄₈O₂Si; In dichloromethane; at 0 ℃; for 0.333333h;

Reference yield:

: 1526930-28-8
1-((3S,10R,13S,17S)-3-((tert-butyldiphenylsilyl)oxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)ethanone

: 1526916-02-8
C₃₇H₄₈Br₂OSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / methanol; toluene / 4 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium periodate / tetrahydrofuran; water

4.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C

4.2: 0.33 h / 0 °C

With sodium periodate; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; toluene;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1526916-02-8
C₃₇H₄₈Br₂OSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / dichloromethane / 4 h / 0 - 20 °C

2.1: boron trifluoride diethyl etherate / methanol; toluene / 4 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium periodate / tetrahydrofuran; water

5.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C

5.2: 0.33 h / 0 °C

With 1H-imidazole; sodium periodate; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; toluene;