C₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃⁽¹⁺⁾*I^(1-)=IC₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃

Base Information

• Chemical Name: C₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃⁽¹⁺⁾*I^(1-)=IC₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃
• CAS No.: 1262802-66-3
• Molecular Formula: C₁₇H₁₉N₄O₄*I
• Molecular Weight: 470.267
• Mol file: 1262802-66-3.mol

Synonyms:C₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃⁽¹⁺⁾*I^(1-)=IC₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃

Chemical Property of C₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃⁽¹⁺⁾*I^(1-)=IC₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃⁽¹⁺⁾*I^(1-)=IC₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃

There total 1 articles about C₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃⁽¹⁺⁾*I^(1-)=IC₅N₄H(O)2(CH₃)3CH₂C₆H₄C(O)OCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.4%

C16H16N4O4 (1262802-65-2) + methyl iodide (74-88-4) → C5N4H(O)2(CH3)3CH2C6H4C(O)OCH3(1+)*I(1-)=IC5N4H(O)2(CH3)3CH2C6H4C(O)OCH3 (1262802-66-3)

Guidance literature:

In N,N-dimethyl-formamide; at 85 ℃; for 24h; Pressure tube;

DOI:10.1016/j.ica.2010.08.008

Reference yield: 93.4%

C5N4H(O)2(CH3)3CH2C6H4C(O)OCH3(1+)*I(1-)=IC5N4H(O)2(CH3)3CH2C6H4C(O)OCH3 (1262802-66-3) + silver(I) acetate (563-63-3) → [Ag(OOCCH3)(C5N4(O)2(CH3)3CH2C6H4C(O)OCH3)]

Guidance literature:

In dichloromethane; byproducts: AgI; Ag(CH3COO) (3.64 mmol) added to soln. of IC5N4H(O)2(CH3)3CH2C6H4C(O)OCH3(1.82 mmol), mixt. stirred for 3 h at room temp.; ppt. filtered off, filtrate concd., hexanes added, ppt. filtered off, stirred in ether for 30 min, filtered; elem. anal.;

DOI:10.1016/j.ica.2010.08.008

upstream raw materials:

C₁₆H₁₆N₄O₄

methyl iodide