6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine

Base Information

Chemical Name:6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine
CAS No.:1254514-67-4
Molecular Formula:C₁₄H₁₄Cl₂N₄O₃
Molecular Weight:357.196
Hs Code.:

Synonyms:6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine

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Technology Process of 6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine

There total 2 articles about 6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 124-42-5
acetamidine hydrochloride

: 211685-71-1
(E)-1-(benzotriazol-1-yl)-3,4,4-trichloro-1-(4-ethoxyphenylamino)-2-nitrobuta-1,3-diene

: 1254514-67-4
6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 16.05h;
DOI:10.1515/znb-2010-0710

Reference yield:

: 156-43-4
4-Ethoxyaniline

: 1254514-67-4
6-(dichloromethyl)-4-(4-ethoxyphenylamino)-2-methyl-5-nitropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 11 h / 0 - 20 °C

2: sodium hydride / tetrahydrofuran; mineral oil / 16.05 h / 0 - 20 °C

With sodium hydride; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1515/znb-2010-0710