di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

Base Information

Chemical Name:di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine
CAS No.:294864-70-3
Molecular Formula:C₄₄H₅₅N₅O₈
Molecular Weight:781.949
Hs Code.:

Synonyms:di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

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Chemical Property of di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

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Technology Process of di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

There total 1 articles about di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 294864-69-0
1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

: 294864-70-3
di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

Guidance literature:: With hydrogenchloride; In dichloromethane; for 0.5h;
DOI:10.1016/S0968-0896(00)00113-9

Reference yield: 67.0%

: 79513-22-7
6-bromo-N-(2-(1,1-dimethylethoxycarbonylamino)ethyl)hexanamide

: 294864-70-3
di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

: 294864-71-4
N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 20h;
DOI:10.1016/S0968-0896(00)00113-9

Reference yield:

: 294864-70-3
di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

: 294864-72-5
N-(2-aminoethyl)-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)aminohexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / K₂CO₃ / dimethylformamide / 20 h / 85 °C

2: 67 percent / HCl gas / CH₂Cl₂ / 0.5 h

With hydrogenchloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; 1: Alkylation / 2: Hydrolysis;
DOI:10.1016/S0968-0896(00)00113-9