1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

Base Information

Chemical Name:1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate
CAS No.:294864-69-0
Molecular Formula:C₄₉H₆₃N₅O₁₀
Molecular Weight:882.067
Hs Code.:

Synonyms:1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

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Chemical Property of 1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

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Technology Process of 1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

There total 1 articles about 1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31139-36-3
dibenzyl dicarbonate

: 294864-68-9
bis-[3-(3-amino-propylamino)-propyl]-carbamic acid tert-butyl ester

: 294864-69-0
1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

Guidance literature:: In tetrahydrofuran; for 36h;
DOI:10.1016/S0968-0896(00)00113-9

Reference yield: 91.0%

: 294864-69-0
1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

: 294864-70-3
di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

Guidance literature:: With hydrogenchloride; In dichloromethane; for 0.5h;
DOI:10.1016/S0968-0896(00)00113-9

Reference yield:

: 294864-69-0
1,1-dimethyl N,N-di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylcarbamate

: 294864-72-5
N-(2-aminoethyl)-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)aminohexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / HCl gas / CH₂Cl₂ / 0.5 h

2: 67 percent / K₂CO₃ / dimethylformamide / 20 h / 85 °C

3: 67 percent / HCl gas / CH₂Cl₂ / 0.5 h

With hydrogenchloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; 1: Hydrolysis / 2: Alkylation / 3: Hydrolysis;
DOI:10.1016/S0968-0896(00)00113-9