N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Base Information

Chemical Name:N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide
CAS No.:294864-71-4
Molecular Formula:C₅₇H₇₉N₇O₁₁
Molecular Weight:1038.29
Hs Code.:

N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Synonyms:N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Suppliers and Price of N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

There total 4 articles about N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 79513-22-7
6-bromo-N-(2-(1,1-dimethylethoxycarbonylamino)ethyl)hexanamide

: 294864-70-3
di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propylamine

: 294864-71-4
N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 20h;
DOI:10.1016/S0968-0896(00)00113-9

Reference yield:

: 22809-37-6
6-bromohexanoyl chloride

: 294864-71-4
N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

2: 67 percent / K₂CO₃ / dimethylformamide / 20 h / 85 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Acylation / 2: Alkylation;
DOI:10.1016/S0968-0896(00)00113-9

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 294864-71-4
N-(2-(1,1-dimethylethoxycarbonylamino)ethyl-6-(di(3-(N-phenylmethoxycarbonyl)-N-(3-(phenylmethoxycarbonylamino)propyl)amino)propyl)amino)hexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2; DMF / CH₂Cl₂ / 0 - 20 °C

2: 68 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3: 67 percent / K₂CO₃ / dimethylformamide / 20 h / 85 °C

With oxalyl dichloride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide; 1: Substitution / 2: Acylation / 3: Alkylation;
DOI:10.1016/S0968-0896(00)00113-9