N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide
CAS No.:1365543-59-4
Molecular Formula:C₁₁H₉F₃N₂O₃S
Molecular Weight:306.265
Hs Code.:

N-[cyclopropyl(4-nitrophenyl)-lambda<sup>4</sup>-sulphanylidene]-2,2,2-trifluoroacetamide

Synonyms:N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Suppliers and Price of N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
N-[Cyclopropyl(4-nitrophenyl)sulphanylidene]-2,2,2-trifluoroacetamide
5g
$ 1133.00

Total 2 raw suppliers

Chemical Property of N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-[Cyclopropyl(4-nitrophenyl)sulphanylidene]-2,2,2-trifluoroacetamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

There total 3 articles about N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 851008-48-5
1-(cyclopropylsulphanyl)-4-nitrobenzene

: 354-38-1
2,2,2-trifluoroacetamide

: 1365543-59-4
N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: 1-(cyclopropylsulphanyl)-4-nitrobenzene; 2,2,2-trifluoroacetamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 5 ℃; for 0.75h; Inert atmosphere; Large scale;

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; In tetrahydrofuran; mineral oil; at 0 - 22 ℃; Reagent/catalyst; Temperature; Solvent; Inert atmosphere; Large scale;
DOI:10.1055/s-0034-1378328

Reference yield:

: 851008-48-5
1-(cyclopropylsulphanyl)-4-nitrobenzene

: 354-38-1
2,2,2-trifluoroacetamide

: 851008-45-2
(R,S)-1-(cyclopropylsulfinyl)-4-nitrobenzene

: 1365543-59-4
N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: With N-Bromosuccinimide; potassium tert-butylate; In methanol; at 20 ℃; Reagent/catalyst; Solvent;
DOI:10.1055/s-0034-1378328

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1365543-59-4
N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 30 °C

1.2: 8 h / 135 - 140 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 5 °C

2.2: 14.25 h / 20 - 25 °C

With sodium hydride; potassium carbonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; mineral oil;