4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

Base Information

Chemical Name:4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt
CAS No.:1399035-82-5
Molecular Formula:C₂H₄O₂*C₁₅H₉F₄N₃
Molecular Weight:367.303
Hs Code.:

Synonyms:4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

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Chemical Property of 4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

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Technology Process of 4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

There total 5 articles about 4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1399035-80-3
N-{2-[4-fluoro-3-(trifluoromethyl)phenyl]-2-oxoethyl}isonicotinamide hydrochloride

: 631-61-8,92206-38-7
ammonium acetate

: 1399035-82-5
4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

Guidance literature:: In acetic acid; at 140 ℃; for 20h;
DOI:10.1055/s-0031-1290371

Reference yield:

: 1082951-17-4
(2-amino-1-(4-fluoro, 3-trifluoromethyl-phenyl)-ethanone) p-toluenesulfonate

: 1399035-82-5
4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / 25 °C

2: acetic acid / 20 h / 140 °C

With triethylamine; In dichloromethane; acetic acid;
DOI:10.1055/s-0031-1290371

Reference yield:

: 37832-54-5,108799-40-2
4-piperidinecarboxylic acid hydrochloride

: 1399035-82-5
4-{4-[4-fluoro-3-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}pyridine acetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / 25 °C

2: acetic acid / 20 h / 140 °C

With triethylamine; In dichloromethane; acetic acid;
DOI:10.1055/s-0031-1290371