2-(3-Chloropropoxy)-1,3-dimethoxybenzene

Base Information

• Chemical Name: 2-(3-Chloropropoxy)-1,3-dimethoxybenzene
• CAS No.: 24251-51-2
• Molecular Formula: C₁₁H₁₅ClO₃
• Molecular Weight: 230.691
• DSSTox Substance ID: DTXSID001275919

Synonyms:2-(3-CHLOROPROPOXY)-1,3-DIMETHOXYBENZENE;24251-51-2;SCHEMBL10459147;DTXSID001275919;AKOS000138366

Chemical Property of 2-(3-Chloropropoxy)-1,3-dimethoxybenzene

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 230.0709720
• Heavy Atom Count: 15
• Complexity: 154

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=C(C(=CC=C1)OC)OCCCCl

Technology Process of 2-(3-Chloropropoxy)-1,3-dimethoxybenzene

There total 2 articles about 2-(3-Chloropropoxy)-1,3-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

1,3-dimethoxy-2-hydroxy-benzene (91-10-1) + 1.3-chlorobromopropane (109-70-6) → 1-Chloro-3-[2,6(dimethoxy)phenoxy]propane (24251-51-2)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Heating;

DOI:10.1021/jm00121a022

Reference yield:

→ 1-Chloro-3-[2,6(dimethoxy)phenoxy]propane (24251-51-2)

Guidance literature:

Reference yield: 40.0%

1-Chloro-3-[2,6(dimethoxy)phenoxy]propane (24251-51-2) + 1,1-bis(4-fluorophenyl)-1-(4-piperidinyl)methanol (60284-98-2) → {1-[3-(2,6-Dimethoxy-phenoxy)-propyl]-piperidin-4-yl}-bis-(4-fluoro-phenyl)-methanol (117023-40-2)

Guidance literature:

With sodium carbonate; potassium iodide; In butan-1-ol; Heating;

DOI:10.1021/jm00121a022

upstream raw materials:

1,3-dimethoxy-2-hydroxy-benzene

1.3-chlorobromopropane

Downstream raw materials:

{1-[3-(2,6-Dimethoxy-phenoxy)-propyl]-piperidin-4-yl}-bis-(4-fluoro-phenyl)-methanol

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