Z-Phe-OBT

Base Information

• Chemical Name: Z-Phe-OBT
• CAS No.: 26055-07-2
• Molecular Formula: C₂₃H₂₀N₄O₄
• Molecular Weight: 416.436

Synonyms:Z-Phe-OBT

Chemical Property of Z-Phe-OBT

Chemical Property:

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Technology Process of Z-Phe-OBT

There total 7 articles about Z-Phe-OBT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-Cbz-L-Phe (1161-13-3) + benzotriazol-1-ol (2592-95-2) → Z-Phe-OBT (26055-07-2)

Guidance literature:

With dmap; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1039/c39850000473

Reference yield:

Cbz-D-Phe (2448-45-5) + benzotriazol-1-ol (2592-95-2) → (R)-2-Benzyloxycarbonylamino-3-phenyl-propionic acid benzotriazol-1-yl ester (26055-07-2)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; for 6h; Ambient temperature;

DOI:10.1039/c39900001045

Reference yield:

N-Cbz-L-Phe (1161-13-3) + 1-methanesulfonyloxy-1,2,3-benzotriazole (54769-22-1) → Z-Phe-OBT (26055-07-2)

Guidance literature:

With triethylamine; In water; ethyl acetate;

upstream raw materials:

Cbz-D-Phe

benzotriazol-1-ol

N-Cbz-L-Phe

1,1-dibenzotriazolo oxallate(DBTO)

Downstream raw materials:

(3S,4S)-3-(2S-2-benzyloxycarbonylamino-2-phenylmethyl-acetamido)-4-acetoxy-azetidin-2-one

Z-Phe-Leu-Arg(Mds)-Arg(Mds)-Ile-Arg(Mds)-Pro-OBut

N-(benzyloxycarbonyl)-L-phenylalanyl-L-phenylalanine methyl ester

ethyl [(2S)-2-(benzyloxycarbonylamino)-3-phenylpropanoylamino]acetate

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