2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide

Base Information

• Chemical Name: 2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide
• CAS No.: 1207088-93-4
• Molecular Formula: C₁₁H₁₁F₅N₄O₂
• Molecular Weight: 326.226

Synonyms:2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide

Chemical Property of 2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide

Chemical Property:

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Technology Process of 2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide

There total 2 articles about 2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3-methyl-4-nitrobenzyl)-hydrazine (866638-96-2) + 2,2,3,3,3-pentafluoro-propionamidine (422-62-8) → 2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide (1207088-93-4)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

(3-methyl-4-nitrobenzyl)-hydrazine (866638-96-2) + 4-methoxybenzyl 2,2,3,3,3-pentafluoropropionimidate → 2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide (1207088-93-4)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 20h;

Reference yield:

2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide (1207088-93-4) + pivaloyl chloride (3282-30-2) → 5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol (1207089-38-0)

Guidance literature:

With sodium hydrogencarbonate; In water; toluene; at 20 ℃; for 2h;

upstream raw materials:

(3-methyl-4-nitrobenzyl)-hydrazine

2,2,3,3,3-pentafluoro-propionamidine

Downstream raw materials:

1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-5-(trifluoromethyl)-4,5-dihydro-1H-1,2,4-triazole

5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

4-{[5,5-dimethyl-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-1-yl]methyl}-2-methylaniline

5-(4-chlorophenyl)-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-1H-1,2,4-triazole

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