5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

Base Information

Chemical Name:5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol
CAS No.:1207089-38-0
Molecular Formula:C₁₆H₁₉F₅N₄O₃
Molecular Weight:410.344
Hs Code.:

Synonyms:5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

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Chemical Property of 5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

Chemical Property:

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Technology Process of 5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

There total 2 articles about 5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207088-93-4
2,2,3,3,3-pentafluoro-N'-(3-methyl-4-nitrobenzyl)propanimide hydrazide

: 3282-30-2
pivaloyl chloride

: 1207089-38-0
5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

Guidance literature:: With sodium hydrogencarbonate; In water; toluene; at 20 ℃; for 2h;

Reference yield:

: 866638-96-2
(3-methyl-4-nitrobenzyl)-hydrazine

: 1207089-38-0
5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 4 h / 20 °C

2: sodium hydrogencarbonate / water; toluene / 2 h / 20 °C

With sodium hydrogencarbonate; In tetrahydrofuran; water; toluene;

Reference yield:

: 1207089-38-0
5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol

: 1207089-39-1
4-{[5-t-butyl-3-(pentafluoroethyl)-1H-1,2,4-triazol-1-yl]methyl}-2-methylaniline

Guidance literature:: 5-t-butyl-1-(3-methyl-4-nitrobenzyl)-3-(pentafluoroethyl)-4,5-dihydro-1H-1,2,4-triazol-5-ol; With hydrogenchloride; tin(II) chloride dihdyrate; In ethanol; water; at 70 ℃; for 1h; Cooling with ice;

With sodium hydroxide; In ethanol; water; pH=11;