C₂₃H₁₉FO₅

Base Information

Chemical Name:C₂₃H₁₉FO₅
CAS No.:1335557-55-5
Molecular Formula:C₂₃H₁₉FO₅
Molecular Weight:394.399
Hs Code.:

C<sub>23</sub>H<sub>19</sub>FO<sub>5</sub>

Synonyms:C₂₃H₁₉FO₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₉FO₅

Chemical Property:

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Technology Process of C₂₃H₁₉FO₅

There total 7 articles about C₂₃H₁₉FO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1335557-55-5
C₂₃H₁₉FO₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: bromine; acetic acid / 2 h / 20 °C

5.1: potassium carbonate / acetone / 3 h / 0 - 50 °C

6.1: lithium diisopropyl amide; diisopropylamine; n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C

6.2: 1 h / -78 - -20 °C

7.1: sodium tetrahydroborate; methanol / 0.67 h

7.2: 1.17 h / -50 - 0 °C / Inert atmosphere

7.3: 1.5 h / 0 - 40 °C

With methanol; sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; bromine; sec.-butyllithium; boron tribromide; potassium carbonate; acetic acid; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1207283-55-3
phenyl 3-fluoro-6-hydroxy-2-methylbenzoate

: 1335557-55-5
C₂₃H₁₉FO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine; acetic acid / 2 h / 20 °C

2.1: potassium carbonate / acetone / 3 h / 0 - 50 °C

3.1: lithium diisopropyl amide; diisopropylamine; n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C

3.2: 1 h / -78 - -20 °C

4.1: sodium tetrahydroborate; methanol / 0.67 h

4.2: 1.17 h / -50 - 0 °C / Inert atmosphere

4.3: 1.5 h / 0 - 40 °C

With methanol; sodium tetrahydroborate; n-butyllithium; bromine; potassium carbonate; acetic acid; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; acetone;

Reference yield:

: 1207283-54-2
phenyl 3-fluoro-6-methoxy-2-methylbenzoate

: 1335557-55-5
C₂₃H₁₉FO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

2.1: bromine; acetic acid / 2 h / 20 °C

3.1: potassium carbonate / acetone / 3 h / 0 - 50 °C

4.1: lithium diisopropyl amide; diisopropylamine; n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C

4.2: 1 h / -78 - -20 °C

5.1: sodium tetrahydroborate; methanol / 0.67 h

5.2: 1.17 h / -50 - 0 °C / Inert atmosphere

5.3: 1.5 h / 0 - 40 °C

With methanol; sodium tetrahydroborate; n-butyllithium; bromine; boron tribromide; potassium carbonate; acetic acid; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; acetone;