C₃₉H₅₈O₅Si₂

Base Information

Chemical Name:C₃₉H₅₈O₅Si₂
CAS No.:289486-27-7
Molecular Formula:C₃₉H₅₈O₅Si₂
Molecular Weight:663.058
Hs Code.:

C<sub>39</sub>H<sub>58</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₉H₅₈O₅Si₂

Suppliers and Price of C₃₉H₅₈O₅Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₅₈O₅Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₅₈O₅Si₂

There total 7 articles about C₃₉H₅₈O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 289486-07-3
1',1'-bis(t-butyldimethylsilyloxymethyl)-1-(4,4'-dimethoxytrityloxy)acetone

: 289486-27-7
C₃₉H₅₈O₅Si₂

Guidance literature:: Methyltriphenylphosphonium bromide; With sodium tert-pentoxide; In diethyl ether; benzene; at 20 ℃; for 5h;

1',1'-bis(t-butyldimethylsilyloxymethyl)-1-(4,4'-dimethoxytrityloxy)acetone; In diethyl ether; benzene; at -10 ℃; for 2h;
DOI:10.1080/15257770008033028

Reference yield:

: 85951-09-3
2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecan-6-ol

: 289486-27-7
C₃₉H₅₈O₅Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: DCC; Py; TFA / dimethylsulfoxide / 24 h / 20 °C

2.1: 34.1 g / methanol / 30 h / 20 °C

3.1: 98 percent / DIBAL-H / diethyl ether / 2 h / -78 °C

4.1: 81 percent / Py / CH₂Cl₂ / 3 h / 20 °C

5.1: BH₃-SMe₂ / tetrahydrofuran / 2 h / 20 °C

5.2: 45 percent / NaBO₃; H₂O₂ / ethanol; H₂O / 0.33 h / 50 °C

6.1: 90 percent / DCC; Py; TFA / dimethylsulfoxide / 5 h / 20 °C

7.1: sodium t-pentoxide / diethyl ether; benzene / 5 h / 20 °C

7.2: 90 percent / diethyl ether; benzene / 2 h / -10 °C

With pyridine; dimethylsulfide borane complex; sodium tert-pentoxide; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; benzene; 1.1: Oxidation / 2.1: Wittig reaction / 3.1: Reduction / 4.1: Substitution / 5.1: Addition / 5.2: Oxidation / 6.1: Oxidation / 7.1: Elimination / 7.2: Wittig reaction;
DOI:10.1080/15257770008033028

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 289486-27-7
C₃₉H₅₈O₅Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: Py / 15 h / 20 °C

2.1: DCC; Py; TFA / dimethylsulfoxide / 24 h / 20 °C

3.1: 34.1 g / methanol / 30 h / 20 °C

4.1: 98 percent / DIBAL-H / diethyl ether / 2 h / -78 °C

5.1: 81 percent / Py / CH₂Cl₂ / 3 h / 20 °C

6.1: BH₃-SMe₂ / tetrahydrofuran / 2 h / 20 °C

6.2: 45 percent / NaBO₃; H₂O₂ / ethanol; H₂O / 0.33 h / 50 °C

7.1: 90 percent / DCC; Py; TFA / dimethylsulfoxide / 5 h / 20 °C

8.1: sodium t-pentoxide / diethyl ether; benzene / 5 h / 20 °C

8.2: 90 percent / diethyl ether; benzene / 2 h / -10 °C

With pyridine; dimethylsulfide borane complex; sodium tert-pentoxide; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; benzene; 1.1: silylation / 2.1: Oxidation / 3.1: Wittig reaction / 4.1: Reduction / 5.1: Substitution / 6.1: Addition / 6.2: Oxidation / 7.1: Oxidation / 8.1: Elimination / 8.2: Wittig reaction;
DOI:10.1080/15257770008033028