4-pentylbenzyl 4-propylphenyl ketone

Base Information

Chemical Name:4-pentylbenzyl 4-propylphenyl ketone
CAS No.:83805-09-8
Molecular Formula:C₂₂H₂₈O
Molecular Weight:308.464
Hs Code.:

Synonyms:4-pentylbenzyl 4-propylphenyl ketone

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Chemical Property of 4-pentylbenzyl 4-propylphenyl ketone

Chemical Property:

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Technology Process of 4-pentylbenzyl 4-propylphenyl ketone

There total 1 articles about 4-pentylbenzyl 4-propylphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6853-58-3
1-(bromomethyl)-4-n-pentylbenzene

: 60484-66-4
p-n-propylbenzonitrile

: 1595-09-1
1-methyl-4-n-pentylbenzene

: 1,2-di-(4-pentylphenyl)ethane

: 83805-09-8
4-pentylbenzyl 4-propylphenyl ketone

Guidance literature:: With magnesium; In diethyl ether; for 5h; Yield given; Ambient temperature;
DOI:10.1002/hlca.19820650423

Reference yield: 95.0%

: 105-36-2
ethyl bromoacetate

: 83805-09-8
4-pentylbenzyl 4-propylphenyl ketone

: 83787-92-2
ethyl 3-hydroxy-4-(4-pentylphenyl)-3-(4-propylphenyl)butyrate

Guidance literature:: With zinc; In benzene; at 70 - 75 ℃; for 2.5h;
DOI:10.1002/hlca.19820650423

Reference yield:

: 83805-09-8
4-pentylbenzyl 4-propylphenyl ketone

: 6-pentyl-2-(4-propylphenyl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / Zn / benzene / 2.5 h / 70 - 75 °C

2: 70percent aq. HClO₄ / acetic acid / 0.17 h / 50 °C / vacuum

3: H₂ / 10percent Pd/C / ethanol / 2 h / Ambient temperature

4: NaOH / H₂O; CH₂Cl₂; methanol / 1.) 50 deg C, 1 h; 2.) 57 deg C, 2 h

5: SOCl₂ / dimethylformamide; toluene / Ambient temperature

6: AlCl₃ / CH₂Cl₂ / 2 h / -50 °C

7: H₂ / 10percent Pd/C / ethanol; dioxane / 3.5 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; thionyl chloride; perchloric acid; hydrogen; zinc; palladium on activated charcoal; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1002/hlca.19820650423