acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

Base Information

Chemical Name:acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique
CAS No.:76146-46-8
Molecular Formula:C₂₇H₃₄N₂O₈
Molecular Weight:514.576
Hs Code.:

Synonyms:acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

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Chemical Property of acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

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Technology Process of acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

There total 3 articles about acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 76146-43-5
(3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoate de methyle

: 76146-46-8
acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

Guidance literature:: With sodium hydroxide; In methanol; water; for 2.5h; Heating;
DOI:10.1016/0040-4020(80)80072-X

Reference yield:

: 76146-53-7,119962-75-3,131903-13-4
lactone de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

: 76146-46-8
acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 4N NaOH / H₂O / 2 h / 20 °C

2: 56 percent / acide p. toluene sulfonique / CHCl₃ / 3 h / 20 °C

3: 93 percent / 1N NaOH / methanol; H₂O / 2.5 h / Heating

With sodium hydroxide; acide p. toluene sulfonique; In methanol; chloroform; water;
DOI:10.1016/0040-4020(80)80072-X

Reference yield:

: 76146-41-3
(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

: 76146-46-8
acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / acide p. toluene sulfonique / CHCl₃ / 3 h / 20 °C

2: 93 percent / 1N NaOH / methanol; H₂O / 2.5 h / Heating

With sodium hydroxide; acide p. toluene sulfonique; In methanol; chloroform; water;
DOI:10.1016/0040-4020(80)80072-X