methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

Base Information

Chemical Name:methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique
CAS No.:76146-54-8
Molecular Formula:C₃₂H₃₈N₄O₈
Molecular Weight:606.676
Hs Code.:

Synonyms:methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

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Chemical Property of methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

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Technology Process of methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

There total 7 articles about methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

: 76146-50-4
methyl-2 (((phenylmethoxy)carbonyl)methyl)-2-hydrazide de l'acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

: 76146-54-8
methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

Guidance literature:: With acetic acid; In water; at 20 ℃; for 4h;
DOI:10.1016/0040-4020(80)80072-X

Reference yield: 14.0%

: tosylate de l'ester benzylique de l'acide 1-methylhydrazinoacetique

: 76146-53-7,119962-75-3,131903-13-4
lactone de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

: 76146-54-8
methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

Guidance literature:: With sodium hydroxide; Kieselgel Merck H ⁽⁶⁰⁾; In water; acetonitrile; at 85 ℃; for 17h;
DOI:10.1016/0040-4020(80)80072-X

Reference yield:

: tosylate de l'ester benzylique de l'acide 1-methylhydrazinoacetique

: 76146-54-8
methyl-2 (((phenylmethoxy)carbonyl)methyl)-2 hydrazide de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / dicyclohexylcarbodiimide / acetonitrile; triethylamine / 6 h / 0 - 20 °C / 1. 2h 0 gradC; 2. 4h 20 gradC

2: 73.5 percent / CH₃COOH / H₂O / 4 h / 20 °C

With acetic acid; dicyclohexyl-carbodiimide; In water; triethylamine; acetonitrile;
DOI:10.1016/0040-4020(80)80072-X