(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

Base Information

Chemical Name:(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle
CAS No.:76146-41-3
Molecular Formula:C₂₃H₂₈N₂O₇
Molecular Weight:444.485
Hs Code.:

Synonyms:(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

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Chemical Property of (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

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Technology Process of (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

There total 1 articles about (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 76146-53-7,119962-75-3,131903-13-4
lactone de l'acide (3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoique

: 76146-41-3
(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

Guidance literature:: With sodium hydroxide; In water; at 20 ℃; for 2h;
DOI:10.1016/0040-4020(80)80072-X

Reference yield: 56.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 76146-41-3
(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

: 76146-43-5
(3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoate de methyle

Guidance literature:: With acide p. toluene sulfonique; In chloroform; at 20 ℃; for 3h;
DOI:10.1016/0040-4020(80)80072-X

Reference yield:

: 76146-41-3
(3RS-5RS) hydroxy-5 bis(((phenylmethoxy)carbonyl)amino)-3,6 hexanoate de methyle

: 76146-46-8
acide (3RS-5RS) bis(((phenylmethoxy)carbonyl)amino)-3,6 (2-(tetrahydropyrannyloxy))-5 hexanoique

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / acide p. toluene sulfonique / CHCl₃ / 3 h / 20 °C

2: 93 percent / 1N NaOH / methanol; H₂O / 2.5 h / Heating

With sodium hydroxide; acide p. toluene sulfonique; In methanol; chloroform; water;
DOI:10.1016/0040-4020(80)80072-X