1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide

Base Information

• Chemical Name: 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide
• CAS No.: 1007580-21-3
• Molecular Formula: Br*C₂₁H₂₇N₂
• Molecular Weight: 387.363
• Mol file: 1007580-21-3.mol

Synonyms:1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide

Chemical Property of 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide

There total 3 articles about 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2BrH*C20H28N2 + trimethyl orthoformate (149-73-5) → 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide (1007580-21-3)

Guidance literature:

With formic acid; at 110 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2009.12.072

Reference yield: 90.0%

N,N'-dimesitylformamidine (75105-48-5) + ethylene dibromide (106-93-4) → 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide (1007580-21-3)

Guidance literature:

With potassium carbonate; In acetonitrile; for 72h; Reflux;

DOI:10.1039/d0ob00036a

Reference yield:

2,4,6-trimethylaniline (88-05-1) → 1,3-bis(2,4,6-trimethylphenyl-1-yl)imidazolidinium dihydrobromide (1007580-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 1 h / Reflux

2: potassium carbonate / acetonitrile / 72 h / Reflux

With potassium carbonate; acetic acid; In acetonitrile;

DOI:10.1039/d0ob00036a

upstream raw materials:

N,N'-dimesitylformamidine

ethylene dibromide

trimethyl orthoformate

2,4,6-trimethylaniline