5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

Base Information

Chemical Name:5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid
CAS No.:946066-41-7
Molecular Formula:C₂₂H₁₈ClNO₅S
Molecular Weight:443.908
Hs Code.:

Synonyms:5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

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Chemical Property of 5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

Chemical Property:

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Technology Process of 5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

There total 1 articles about 5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 88-53-9
5-amino-2-chloro-toluene-4-sulfonic acid

: 946066-41-7
5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; at 0 ℃;

Reference yield:

: 946066-41-7
5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

: 910577-02-5
(4-chloro-2-chlorosulfonyl-5-methyl-phenyl)-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/jm060168g

Reference yield:

: 946066-41-7
5-chloro-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-benzenesulfonic acid

: 1-[(2-amino-5-chloro-4-methylphenyl)sulfonyl]-L-proline

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 4 h / 20 °C

With thionyl chloride; In N,N-dimethyl-formamide;
DOI:10.1021/jm060168g