N¹-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N¹-methyl-heptane-1,7-diamine

Base Information

• Chemical Name: N¹-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N¹-methyl-heptane-1,7-diamine
• CAS No.: 110231-06-6
• Molecular Formula: C₂₃H₃₆N₄O
• Molecular Weight: 384.565

Synonyms:N¹-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N¹-methyl-heptane-1,7-diamine

Chemical Property of N¹-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N¹-methyl-heptane-1,7-diamine

Chemical Property:

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Technology Process of N¹-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N¹-methyl-heptane-1,7-diamine

There total 3 articles about N¹-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N¹-methyl-heptane-1,7-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile (109912-35-8) → N1-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N1-methyl-heptane-1,7-diamine (110231-06-6)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 22 ℃; for 18h;

DOI:10.1016/0223-5234(87)90002-X

Reference yield:

N'-formyl-N-(4-methoxybenzyl)-N-2-pyridinyl-1,2-ethanediamine (109912-29-0) → N1-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N1-methyl-heptane-1,7-diamine (110231-06-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

2: potassium carbonate / dimethylformamide / 2 h / 100 °C

3: LiAlH₄ / diethyl ether / 18 h / 22 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;

DOI:10.1016/0223-5234(87)90002-X

Reference yield:

N-(4-methoxybenzyl)-N-2-pyridinyl-1,2-ethanediamine (109912-28-9) → N1-{2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-N1-methyl-heptane-1,7-diamine (110231-06-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / acetic anhydride / diethyl ether / 16 h / 22 °C

2: 95 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

3: potassium carbonate / dimethylformamide / 2 h / 100 °C

4: LiAlH₄ / diethyl ether / 18 h / 22 °C

With lithium aluminium tetrahydride; acetic anhydride; potassium carbonate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;

DOI:10.1016/0223-5234(87)90002-X

upstream raw materials:

7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

N'-formyl-N-(4-methoxybenzyl)-N-2-pyridinyl-1,2-ethanediamine

N-(4-methoxybenzyl)-N-2-pyridinyl-1,2-ethanediamine

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