N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

Base Information

Chemical Name:N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide
CAS No.:205258-08-8
Molecular Formula:C₂₂H₂₅N₇O₂S
Molecular Weight:451.552
Hs Code.:

Synonyms:N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

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Chemical Property of N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

Chemical Property:

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Technology Process of N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

There total 4 articles about N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 622-78-6
Benzyl isothiocyanate

: 205259-32-1
7-(ethylamino)-6-nitro-4-(1-piperazinyl)quinazoline

: 205258-08-8
N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

Guidance literature:: DOI:10.1021/jm020505v

Reference yield:

: 53449-14-2
7-chloro-6-nitro-4(3H)-quinazolinone

: 205258-08-8
N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylsulfoxide / 180 °C

2: POCl₃ / Heating

3: propan-2-ol / 4 h / Heating

With trichlorophosphate; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1021/jm020505v

Reference yield:

: 168761-50-0
7-(ethylamino)-6-nitroquinazoline-4(3H)-one

: 205258-08-8
N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃ / Heating

2: propan-2-ol / 4 h / Heating

With trichlorophosphate; In isopropyl alcohol;
DOI:10.1021/jm020505v