4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

Base Information

Chemical Name:4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide
CAS No.:205259-13-8
Molecular Formula:C₂₂H₂₇N₇S
Molecular Weight:421.569
Hs Code.:

Synonyms:4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

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Chemical Property of 4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

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Technology Process of 4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

There total 6 articles about 4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 205258-08-8
N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

: 205259-13-8
4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

Guidance literature:: With iron(III) chloride; iron; In ethanol; water; for 4h; Heating;
DOI:10.1021/jm020505v

Reference yield: 92.0%

: iron (III) chloride hexahydrate

: 7439-89-6
iron

: 205258-08-8
N-benzyl-4-(7-ethylamino-6-nitro-4-quinazolinyl)-1-piperazinethiocarboxamide

: 205259-13-8
4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

Guidance literature:: In ethanol; water;

Reference yield:

: 53449-14-2
7-chloro-6-nitro-4(3H)-quinazolinone

: 205259-13-8
4-(6-amino-7-ethylamino-4-quinazolinyl)-N-benzyl-1-piperazinethiocarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylsulfoxide / 180 °C

2: POCl₃ / Heating

3: propan-2-ol / 4 h / Heating

4: 92 percent / Fe; FeCl₃*6H₂O / ethanol; H₂O / 4 h / Heating

With iron(III) chloride; iron; trichlorophosphate; In ethanol; water; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1021/jm020505v