ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

Base Information

Chemical Name:ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate
CAS No.:831223-28-0
Molecular Formula:C₃₁H₃₉FO₄SeSi
Molecular Weight:601.692
Hs Code.:

Synonyms:ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

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Chemical Property of ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

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Technology Process of ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

There total 3 articles about ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 831223-27-9
2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenol

: 105-36-2
ethyl bromoacetate

: 831223-28-0
ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

Guidance literature:: With potassium carbonate; In acetonitrile; for 3h;
DOI:10.1021/ol048053z

Reference yield:

: 2105-94-4
4-bromo-2-fluorophenol

: 831223-28-0
ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-BuLi / tetrahydrofuran / 0.33 h / -78 °C

1.2: Se / tetrahydrofuran / 1 h / 20 °C

1.3: 97 percent / tetrahydrofuran / 0 - 20 °C

2.1: 97 percent / K₂CO₃ / acetonitrile / 3 h

With tert.-butyl lithium; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol048053z

Reference yield:

: 164025-54-1
tert-butyl-(5-iodo-pentyloxy)-diphenyl-silane

: 831223-28-0
ethyl 2-fluoro-4-[5-(tert-butyldiphenylsilanyloxy)-pentylselanyl]-phenyloxyacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-BuLi / tetrahydrofuran / 0.33 h / -78 °C

1.2: Se / tetrahydrofuran / 1 h / 20 °C

1.3: 97 percent / tetrahydrofuran / 0 - 20 °C

2.1: 97 percent / K₂CO₃ / acetonitrile / 3 h

With tert.-butyl lithium; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol048053z