<(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

Base Information

Chemical Name:<(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane
CAS No.:217640-33-0
Molecular Formula:C₁₄H₁₂INO₂S
Molecular Weight:385.225
Hs Code.:

<(ethenylphenylsulfonyl)imino>phenyl-λ<sup>3</sup>-iodane

Synonyms:<(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

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Technology Process of <(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

There total 4 articles about <(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 51119-84-7
2-ethenylbenzenesulfonamide

: 217640-33-0
<(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 3h;
DOI:10.1139/cjc-76-6-738

Reference yield:

: 2512-24-5
N-tert-butylbenzenesulfonamide

: 217640-33-0
<(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 3 h / -60 - -20 °C

1.2: tetrahydrofuran; hexane / 0.08 h / 0 °C

2.1: 1.89 g / potassium tert-butoxide / tetrahydrofuran; hexane / 2 h / 20 °C

3.1: 94 percent / trifluoroacetic acid; anisole / 24 h / 0 °C

4.1: potassium hydroxide / methanol / 0 - 5 °C

With potassium hydroxide; n-butyllithium; potassium tert-butylate; methoxybenzene; trifluoroacetic acid; In tetrahydrofuran; methanol; hexane; 1.1: Metallation / 1.2: Formylation / 2.1: Wittig reaction / 3.1: deprotection / 4.1: Condensation;
DOI:10.1021/ol000130c

Reference yield:

: 156359-40-9
N-tert-Butyl-2-formyl-benzenesulfonamide

: 217640-33-0
<(ethenylphenylsulfonyl)imino>phenyl-λ³-iodane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.89 g / potassium tert-butoxide / tetrahydrofuran; hexane / 2 h / 20 °C

2: 94 percent / trifluoroacetic acid; anisole / 24 h / 0 °C

3: potassium hydroxide / methanol / 0 - 5 °C

With potassium hydroxide; potassium tert-butylate; methoxybenzene; trifluoroacetic acid; In tetrahydrofuran; methanol; hexane; 1: Wittig reaction / 2: deprotection / 3: Condensation;
DOI:10.1021/ol000130c