(+)-(1R,2S)-cis-1-(4-methylphenyl)-2-phenylethylene oxide

Base Information

Chemical Name:(+)-(1R,2S)-cis-1-(4-methylphenyl)-2-phenylethylene oxide
CAS No.:62137-65-9
Molecular Formula:C₁₅H₁₄O
Molecular Weight:210.276
Hs Code.:

Synonyms:(+)-(1R,2S)-cis-1-(4-methylphenyl)-2-phenylethylene oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(1R,2S)-cis-1-(4-methylphenyl)-2-phenylethylene oxide

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Technology Process of (+)-(1R,2S)-cis-1-(4-methylphenyl)-2-phenylethylene oxide

There total 60 articles about (+)-(1R,2S)-cis-1-(4-methylphenyl)-2-phenylethylene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-52-7
benzaldehyde

: p-methylbenzaldehyde tosylhydrazone sodium salt

: 22440-35-3,28291-09-0,36044-60-7,36084-19-2,42730-01-8,58770-05-1,62137-65-9,66701-17-5,70332-46-6
trans-2-(4-methylbenzenyl)-3-phenyl-oxirane

Guidance literature:: With triphenyl-arsane; N-benzyl-N,N,N-triethylammonium chloride; dirhodium tetraacetate; In acetonitrile; at 40 ℃;
DOI:10.1039/b204252e

Reference yield: 97.0%

: 123-11-5
4-methoxy-benzaldehyde

: sodium (E)-2-benzylidene-1-tosylhydrazin-1-ide

: 22440-35-3,28291-09-0,36044-60-7,36084-19-2,42730-01-8,58770-05-1,62137-65-9,66701-17-5,70332-46-6
trans-2-(4-methylbenzenyl)-3-phenyl-oxirane

Guidance literature:: With thiophene; dirhodium tetraacetate; N-benzyl-N,N,N-triethylammonium chloride; In acetonitrile; at 40 ℃; for 24h;
DOI:10.1021/ja034606+

Reference yield: 91.0%

: 104-81-4
4-Methylbenzyl bromide

: 100-51-6,185532-71-2
benzyl alcohol

: 22440-35-3,28291-09-0,36044-60-7,36084-19-2,42730-01-8,58770-05-1,62137-65-9,66701-17-5,70332-46-6
trans-2-(4-methylbenzenyl)-3-phenyl-oxirane

Guidance literature:: benzyl alcohol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h; Inert atmosphere;

4-Methylbenzyl bromide; With N-ethyl-N,N-diisopropylamine; potassium hydroxide; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.joc.9b02621