3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

Base Information

Chemical Name:3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine
CAS No.:1232359-39-5
Molecular Formula:C₂₅H₃₆N₂O₇Si
Molecular Weight:504.656
Hs Code.:

Synonyms:3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

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Chemical Property of 3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

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Technology Process of 3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

There total 4 articles about 3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1232359-36-2
3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-ethoxycarbonylmethylribosylthymine

: 1232359-39-5
3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

Guidance literature:: 3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-ethoxycarbonylmethylribosylthymine; With potassium hydroxide; In ethanol; for 1h;

With potassium hydrogensulfate; In ethanol; water;
DOI:10.1134/S1068162010020093

Reference yield:

: 1204744-83-1
2'-O-acetyl-3'-O-benzyl-5'-deoxy-5'-ethoxycarbonylmethyl-5-methyluridine

: 1232359-39-5
3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; potassium carbonate / 4 h

1.2: 0.08 h

2.1: 1H-imidazole / acetonitrile

3.1: potassium hydroxide / ethanol / 1 h

With 1H-imidazole; methanol; potassium carbonate; potassium hydroxide; In ethanol; acetonitrile;
DOI:10.1134/S1068162010020093

Reference yield:

: 1232359-33-9
3'-O-benzyl-5'-deoxy-5'-ethoxycarbonylmethylribosylthymine

: 1232359-39-5
3'-O-benzyl-2'-O-tert-butyldimethylsilyl-5'-deoxy-5'-carboxymethylribosylthymine

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / acetonitrile

2: potassium hydroxide / ethanol / 1 h

With 1H-imidazole; potassium hydroxide; In ethanol; acetonitrile;
DOI:10.1134/S1068162010020093