(Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

Base Information

Chemical Name:(Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone
CAS No.:1422525-09-4
Molecular Formula:C₂₅H₂₃NO₃
Molecular Weight:385.463
Hs Code.:

Synonyms:(Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

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Chemical Property of (Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

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Technology Process of (Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

There total 2 articles about (Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 67-56-1
methanol

: 1422524-90-0
(Z)-2-(2-hydroxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

: 1422525-09-4
(Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

Guidance literature:: With hydroxylamine hydrochloride; copper(II) oxide; Reflux;
DOI:10.1016/j.tet.2012.12.060

Reference yield:

: 667881-74-5
2-(methylthio)-1,4-dip-tolylbut-2-ene-1,4-dione

: 95-55-6
2-amino-phenol

: 1422525-09-4
(Z)-2-(2-methoxy-2-p-tolyl-2H-benzo[b][1,4]oxazin-3(4H)-ylidene)-1-p-tolylethanone

Guidance literature:: Multi-step reaction with 2 steps

1: tert-butyl alcohol / 12 h / Reflux

2: hydroxylamine hydrochloride; copper(II) oxide / Reflux

With hydroxylamine hydrochloride; copper(II) oxide; In tert-butyl alcohol;
DOI:10.1016/j.tet.2012.12.060