methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

Base Information

Chemical Name:methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate
CAS No.:20365-71-3
Molecular Formula:C₁₁H₁₂O₂S₂
Molecular Weight:240.347
Hs Code.:

Synonyms:methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

Suppliers and Price of methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

There total 3 articles about methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2314-48-9
(S,S)-dimethyl trithiocarbonate

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 20365-71-3
methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

Guidance literature:: 1-(4-methoxyphenyl)ethanone; With sodium hydride; In hexane; N,N-dimethyl-formamide; for 1h; Cooling with ice; Inert atmosphere;

(S,S)-dimethyl trithiocarbonate; at 20 ℃; for 8h;
DOI:10.1039/c4dt03816a

Reference yield: 21.7%

: 75-15-0,12122-00-8
carbon disulfide

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 74-88-4
methyl iodide

: 20365-71-3
methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

Guidance literature:: carbon disulfide; 1-(4-methoxyphenyl)ethanone; With potassium tert-butylate; In diethyl ether; at 0 ℃; for 1.5h; Inert atmosphere;

methyl iodide; In diethyl ether; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2014.07.023