2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

Base Information

Chemical Name:2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester
CAS No.:1609182-72-0
Molecular Formula:C₁₁H₁₁NO₃S₂
Molecular Weight:269.345
Hs Code.:

Synonyms:2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

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Chemical Property of 2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

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Technology Process of 2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

There total 3 articles about 2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 213468-59-8
S-methyl 3-oxo-3-(4-methoxylphenyl)propanedithioate

: 1609182-72-0
2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

Guidance literature:: With hydrogenchloride; sodium nitrite; In methanol; at 0 ℃; for 25h; Inert atmosphere;
DOI:10.1021/acs.joc.7b01601

Reference yield: 70.0%

: 20365-71-3
methyl 3-hydroxy-3-(p-methoxyphenyl)-2-propenedithiolate

: 1609182-72-0
2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

Guidance literature:: With hydrogenchloride; sodium nitrite; In methanol; for 0.666667h; Cooling with ice;
DOI:10.1016/j.tet.2014.03.097

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1609182-72-0
2-hydroxyimino-3-(4-methoxy-phenyl)-3-oxo-dithiopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: hydrogenchloride; sodium nitrite / methanol / 25 h / 0 °C / Inert atmosphere

With hydrogenchloride; sodium hydride; sodium nitrite; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/acs.joc.7b01601