N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

Base Information

Chemical Name:N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine
CAS No.:503612-98-4
Molecular Formula:C₂₆H₂₁F₃N₆O₃
Molecular Weight:522.486
Hs Code.:

Synonyms:N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

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Chemical Property of N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

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Technology Process of N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

There total 4 articles about N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₁₆F₃N₅O₂

: 593-56-6
N-methoxylamine hydrochloride

: 503612-98-4
N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

Guidance literature:: C₂₅H₁₆F₃N₅O₂; With hydrogenchloride; methanol; at 20 ℃; for 24h;

N-methoxylamine hydrochloride; With triethylamine; In methanol; at 20 ℃; for 24h;

Reference yield:

: 574012-03-6
O-methoxy-hydroxylamine hydrochloride

: 503612-97-3
N-hydroxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydropyrazolo[3,4-c]pyridin-1-yl}benzamidine

: 503612-98-4
N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

Guidance literature:: With triethylamine; In methanol;

Reference yield:

: 385425-17-2
3-[6-(4-iodophenyl)-7-oxo-3-trifluoromethyl-4,5,6,7-tetrahydropyrazolo[3,4-c]pyridin-1-yl]benzonitrile

: 503612-98-4
N-methoxy-3-{7-oxo-6-[4-(2-oxo-2H-pyridin-1-yl)-phenyl]-3-trifluoromethyl-4,5,6,7-tetrahydro-pyrazolo[3,4-c]pyridin-1-yl}-benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; copper(l) iodide / 18 h / Reflux

2.1: hydrogenchloride; methanol / 24 h / 20 °C

2.2: 24 h / 20 °C

With hydrogenchloride; methanol; copper(l) iodide; potassium carbonate;