2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

Base Information

Chemical Name:2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol
CAS No.:1333501-15-7
Molecular Formula:C₂₇H₄₇NO₆
Molecular Weight:481.673
Hs Code.:

Synonyms:2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

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Chemical Property of 2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

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Technology Process of 2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

There total 5 articles about 2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1333501-33-9
4-[2-(2-{2-[2-(tert-butyldimethylsilyloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine

: 1333501-15-7
2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

Guidance literature:: With pyridine; hydrogen fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201100543

Reference yield:

: 77544-60-6
p-toluenesulfonic acid 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester

: 1333501-15-7
2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 0 - 60 °C / Inert atmosphere

3.1: copper(II) trifluoroacetate; copper; 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 72 h / 75 °C / Inert atmosphere

4.1: pyridine; hydrogen fluoride / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogen fluoride; copper(II) trifluoroacetate; copper; sodium hydride; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201100543

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1333501-15-7
2-[2-(2-{2-[2,2,6,6-tetramethyl-1-(2-methyl-1-phenylpropoxy)piperidine-4-yloxy]ethoxy}ethoxy)ethoxy]ethanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 0 - 60 °C / Inert atmosphere

4.1: copper(II) trifluoroacetate; copper; 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 72 h / 75 °C / Inert atmosphere

5.1: pyridine; hydrogen fluoride / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogen fluoride; copper(II) trifluoroacetate; copper; sodium hydride; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201100543