4-nitro-N-[(E)-[(2E)-2-[(4-nitrophenyl)hydrazinylidene]ethylidene]amino]aniline

Base Information

• Chemical Name: 4-nitro-N-[(E)-[(2E)-2-[(4-nitrophenyl)hydrazinylidene]ethylidene]amino]aniline
• CAS No.: 3078-13-5
• Molecular Formula: C14H12N6O4
• Molecular Weight: 328.287
• NSC Number: 406805
• Mol file: 3078-13-5.mol

Synonyms:NSC406805;NSC-406805;3078-13-5

Chemical Property of 4-nitro-N-[(E)-[(2E)-2-[(4-nitrophenyl)hydrazinylidene]ethylidene]amino]aniline

Chemical Property:

• Boiling Point: 533.1°Cat760mmHg
• Flash Point: 276.2°C
• Density: 1.42g/cm³
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 5
• Exact Mass: 328.09200289
• Heavy Atom Count: 24
• Complexity: 427

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1NN=CC=NNC2=CC=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]
• Isomeric SMILES: C1=CC(=CC=C1N/N=C/C=N/NC2=CC=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 4-nitro-N-[(E)-[(2E)-2-[(4-nitrophenyl)hydrazinylidene]ethylidene]amino]aniline

There total 6 articles about 4-nitro-N-[(E)-[(2E)-2-[(4-nitrophenyl)hydrazinylidene]ethylidene]amino]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Glyoxal (131543-46-9,107-22-2) + 4-nitrophenylhydrazone (100-16-3) → glyoxal bis-(4-nitrophenylhydrazone) (3078-13-5)

Guidance literature:

With acetic acid;

Reference yield:

Glycolaldehyde (141-46-8) + 4-nitrophenylhydrazone (100-16-3) → glycolaldehyde-(4-nitro-phenylhydrazone) (68044-21-3) + glyoxal bis-(4-nitrophenylhydrazone) (3078-13-5)

Guidance literature:

With ethanol;

Reference yield:

l-canavanine (543-38-4,13269-28-8) → glyoxal bis-(4-nitrophenylhydrazone) (3078-13-5)

Guidance literature:

dann Umsetzung mit 4-Nitro-phenylhydrazin in essigsaurer Loesung;

upstream raw materials:

ethanol

2,2,2-tribromoethanol

sodium acetate

acetic acid

Downstream raw materials:

N,N'-di-(4-nitrophenyl)oxalodihydrazonyl dibromide

6-nitrocinnolin-4-ylamine

4,4'-Bis-(4-nitro-phenyl)-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine

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