(3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide

Base Information

• Chemical Name: (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide
• CAS No.: 171270-54-5
• Molecular Formula: C₃₄H₅₆N₂O₇
• Molecular Weight: 604.828

Synonyms:(3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide

Chemical Property of (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide

Chemical Property:

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Technology Process of (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide

There total 4 articles about (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-hydroxyhexadecanamide + (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate (56602-33-6) + Nα-tert-butyloxycarbonyl-L-homoglutamic acid δ-benzyl ester (37051-23-3,80975-50-4,112295-37-1) → (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide (171270-54-5)

Guidance literature:

With dmap; In dichloromethane; ethyl acetate;

Reference yield:

(S)-β-hydroxyhexadecanoic acid methyl ester (76898-45-8) + benzyl bromide (100-39-0) → (S)-benzyl 3-hydroxyhexadecanoate + (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide (171270-54-5)

Guidance literature:

Reference yield:

(S)-β-hydroxyhexadecanoic acid methyl ester (76898-45-8) + 1,1,1-trichloroethanol (115-20-8) → (S)-(2,2,2-trichloroethyl) 3-hydroxyhexadecanoate (171272-19-8) + (3S)-3-[(2S)-5-benzyloxycarbonyl-2-(tertiarybutoxycarbonylamino)-pentanoyl]oxyhexadecanamide (171270-54-5)

Guidance literature:

upstream raw materials:

(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate

N^α-tert-butyloxycarbonyl-L-homoglutamic acid δ-benzyl ester

(S)-β-hydroxyhexadecanoic acid methyl ester

benzyl bromide

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