5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

Base Information

Chemical Name:5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine
CAS No.:911062-06-1
Molecular Formula:C₁₆H₁₅BrN₄O₂
Molecular Weight:375.225
Hs Code.:

Synonyms:5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

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Chemical Property of 5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

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Technology Process of 5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

There total 4 articles about 5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 6628-77-9
6-methoxy-pyridin-3-ylamine

: 911061-96-6
2-(4-bromophenyl)-5-(methoxymethyl)-1,3,4-oxadiazole

: 911062-06-1
5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

Guidance literature:: With toluene-4-sulfonic acid; In xylene; at 140 ℃; for 18h;

Reference yield:

: 5933-32-4
4-bromobenzoic acid hydrazide

: 911062-06-1
5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C

2: trichlorophosphate / 3 h / 110 °C

3: methanol / 20 h / 20 °C

4: toluene-4-sulfonic acid / xylene / 18 h / 140 °C

With toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; trichlorophosphate; In methanol; dichloromethane; xylene;

Reference yield:

: 568544-04-7
2-(4-bromophenyl)-5-(chloromethyl)-1,3,4-oxadiazole

: 911062-06-1
5-[3-(4-bromophenyl)-5-(methoxymethyl)-4H-1,2,4-triazol-4-yl]-2-methoxypyridine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 20 h / 20 °C

2: toluene-4-sulfonic acid / xylene / 18 h / 140 °C

With toluene-4-sulfonic acid; In methanol; xylene;