Li(Et₂O)2NMesBMes₂

Base Information

Chemical Name:Li(Et₂O)2NMesBMes₂
CAS No.:124855-16-9
Molecular Formula:C₃₅H₅₃BLiNO₂
Molecular Weight:537.563
Hs Code.:

Li(Et<sub>2</sub>O)2NMesBMes<sub>2</sub>

Synonyms:Li(Et₂O)2NMesBMes₂

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Chemical Property of Li(Et₂O)2NMesBMes₂

Chemical Property:

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Technology Process of Li(Et₂O)2NMesBMes₂

There total 3 articles about Li(Et₂O)2NMesBMes₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 109151-64-6
HNMesBMes₂

: 60-29-7,927820-24-4
diethyl ether

: 124855-16-9
Li(Et₂O)2NMesBMes₂

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; addn. of BuLi in hexane to HNMesBMes2 in Et2O cooled in ice bath, stirring 30 min. (N2); filtration, evapn., cooling to -20°C for 12 h, crystn.;

Reference yield:

: 109151-64-6
HNMesBMes₂

: 124855-16-9
Li(Et₂O)2NMesBMes₂

Guidance literature:: With t-BuLi; Et₂O; In tetrahydrofuran; diethyl ether; protective gas: nitrogen; dropwise addn. of t-BuLi (syringe/hexane soln.) to stirred soln. (0°C/1 h);; not isolated;;
DOI:10.1021/ja00250a016

Reference yield:

: 436-59-9
dimesitylfluoroborane

: 124855-16-9
Li(Et₂O)2NMesBMes₂

Guidance literature:: Multi-step reaction with 2 steps

1: LiN(H)C₆H₂(CH₃)3 / diethyl ether

2: t-BuLi; Et₂O / tetrahydrofuran; diethyl ether

With LiN(H)C₆H₂(CH₃)3; t-BuLi; Et₂O; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00250a016