5,15-bis(3,5-di-tert-butylphenyl)porphyrin Zn^II

Base Information

• Chemical Name: 5,15-bis(3,5-di-tert-butylphenyl)porphyrin Zn^II
• CAS No.: 187387-14-0
• Molecular Formula: C₄₈H₅₂N₄Zn
• Molecular Weight: 750.358

Synonyms:5,15-bis(3,5-di-tert-butylphenyl)porphyrin Zn^II

Chemical Property of 5,15-bis(3,5-di-tert-butylphenyl)porphyrin Zn^II

Chemical Property:

Purity/Quality:

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Technology Process of 5,15-bis(3,5-di-tert-butylphenyl)porphyrin Zn^II

There total 2 articles about 5,15-bis(3,5-di-tert-butylphenyl)porphyrin Zn^II which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

zinc(II) acetate dihydrate (5970-45-6) + 5,15-bis(3',5'-di-tert-butylphenyl)porphyrin → [5,15-bis-(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (187387-14-0)

Guidance literature:

In methanol; chloroform; at 65 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.201402634

Reference yield:

5,15-bis(3',5'-di-tert-butylphenyl)porphyrin → [5,15-bis-(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (187387-14-0)

Guidance literature:

With zinc diacetate; In methanol; dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo201490y

Reference yield: 99.0%

silver(I) nitrite (7783-99-5) + [5,15-bis-(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) (187387-14-0) → [5,15-bis(3',5'-di-tert-butylphenyl)-10-(nitro)porphyrinato]zinc(II) (187387-21-9)

Guidance literature:

In not given;

DOI:10.1002/anie.199701351

upstream raw materials:

zinc(II) acetate dihydrate

Downstream raw materials:

Zinc(II) 5,15-di(3,5-di-tert-butylphenyl)porphyrin meso-meso trimer

μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

[5,15-bis(3',5'-di-tert-butylphenyl)-10-(nitro)porphyrinato]zinc(II)

[(NCCHCHCC(C₆H₃(C(CH₃)3)2))2(NCCHCHCC(O))2Zn]

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