μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

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Chemical Name:μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)
CAS No.:187387-16-2
Molecular Formula:C₉₆H₁₀₂N₈Zn₂
Molecular Weight:1498.7
Hs Code.:

Synonyms:μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

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Chemical Property of μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

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Technology Process of μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

There total 6 articles about μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: [5,15-bis[3,5-di(tert-butyl)phenyl]porphyrinato(2-)-κN(21),κN(22),κN(23),κN(24)]zinc(II)

: 187387-17-3
Zinc(II) 5,15-di(3,5-di-tert-butylphenyl)porphyrin meso-meso trimer

: 187387-16-2
μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

: [5,15-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) tetramer

Guidance literature:: With AgPF₆; In chloroform; acetonitrile; N2 atm.; 0.8 equiv of AgPF6, CH3CN/CHCl3 1:4, 25°C, 16 h;
DOI:10.1002/hlca.200590144

Reference yield: 25.0%

: 187387-14-0
[5,15-bis-(3,5-di-tert-butylphenyl)porphyrinato]zinc(II)

: 557-34-6
zinc diacetate

: 187387-17-3
Zinc(II) 5,15-di(3,5-di-tert-butylphenyl)porphyrin meso-meso trimer

: 187387-16-2
μ-[10,10',20,20'-tetrakis[3,5-di(tert-butyl)phenyl]-5,5'-biporphyrinato(4-)-κN(21),κN(22),κN(23),κN(24),κN(21'),κN(22'),κN(23'),.kappaN(24')]dizinc(II)

: [5,15-bis(3,5-di-tert-butylphenyl)porphyrinato]zinc(II) tetramer

Guidance literature:: With silver(I) hexafluorophosphate; In acetonitrile; stirring porphyrin with 0.5 equiv. AgPF6 (0.5 h, room temp., in dark), filtration, water addn., extn. into CHCl3, washing (water), drying (Na2SO4), Zn(OAc)2 addn., refluxing for 1 h; water addn., extn. into CHCl3, washing (water), drying (Na2SO4), repeated chromy. (Bio-Beads SX-1, C6H6);
DOI:10.1002/anie.199701351