9h-Carbazol-9-ylmethyl acetate

Base Information

• Chemical Name: 9h-Carbazol-9-ylmethyl acetate
• CAS No.: 6510-71-0
• Molecular Formula: C15H13NO2
• Molecular Weight: 239.274
• NSC Number: 132289
• DSSTox Substance ID: DTXSID00299715
• Wikidata: Q82042244
• Mol file: 6510-71-0.mol

Synonyms:9h-carbazol-9-ylmethyl acetate;6510-71-0;NSC132289;Oprea1_770910;SCHEMBL18034628;DTXSID00299715;STL327401;AKOS003654009;NSC-132289

Chemical Property of 9h-Carbazol-9-ylmethyl acetate

Chemical Property:

• Vapor Pressure: 8.54E-05mmHg at 25°C
• Boiling Point: 340.5°Cat760mmHg
• Flash Point: 159.8°C
• Density: 1.18g/cm³
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 239.094628657
• Heavy Atom Count: 18
• Complexity: 296

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCN1C2=CC=CC=C2C3=CC=CC=C31

Technology Process of 9h-Carbazol-9-ylmethyl acetate

There total 2 articles about 9h-Carbazol-9-ylmethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.26%

N-hydroxymethylenecarbazole (2409-36-1) + acetic anhydride (108-24-7) → N-acetoxymethylenecarbazole (6510-71-0)

Guidance literature:

With acetic acid; Heating;

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → N-acetoxymethylenecarbazole (6510-71-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 68.8 percent / aq. NaOH / ethanol

2: 7.26 percent / AcOH / Heating

With sodium hydroxide; acetic acid; In ethanol;

Reference yield:

N-acetoxymethylenecarbazole (6510-71-0) → N-ethylcarbazole (86-28-2)

Guidance literature:

With methyl magnesium iodide; diethyl ether;

upstream raw materials:

N-hydroxymethylenecarbazole

acetic anhydride

9H-carbazole

Downstream raw materials:

N-ethylcarbazole

9-propyl 9H-carbazole

9-benzyl-9H-carbazole