N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide
CAS No.:115306-77-9
Molecular Formula:C₁₆H₂₉NO₃SSi
Molecular Weight:343.563
Hs Code.:
DSSTox Substance ID:DTXSID701136908

Synonyms:DTXSID701136908;N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide;115306-77-9

Suppliers and Price of N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:343.16374150
Heavy Atom Count:22
Complexity:429

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NCCCO[Si](C)(C)C(C)(C)C

Technology Process of N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide

There total 5 articles about N-[3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]propyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13379-98-1
3-[N-(4-methylphenylsulfonyl)amino]propan-1-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 115306-77-9
N-<3-(tert-butyldimethylsiloxy)propyl>-p-toluenesulfonamide

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 0 ℃; for 2.5h;
DOI:10.1021/ja073614d

Reference yield: 93.0%

: 115306-75-7
3-(tertbutyldimethylsiloxyl)propylamine

: 98-59-9
p-toluenesulfonyl chloride

: 115306-77-9
N-<3-(tert-butyldimethylsiloxy)propyl>-p-toluenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ja00225a032

Reference yield: 89.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 98-59-9
p-toluenesulfonyl chloride

: 156-87-6
propan-1-ol-3-amine

: 115306-77-9
N-<3-(tert-butyldimethylsiloxy)propyl>-p-toluenesulfonamide

Guidance literature:: tert-butyldimethylsilyl chloride; propan-1-ol-3-amine; With 1H-imidazole; In dichloromethane; at 20 ℃;

p-toluenesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1002/anie.201700596