N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

Base Information

Chemical Name:N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide
CAS No.:192126-71-9
Molecular Formula:C₄₈H₃₈N₂O₆
Molecular Weight:738.84
Hs Code.:

Synonyms:N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

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Chemical Property of N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

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Technology Process of N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

There total 3 articles about N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 191997-95-2
N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride

: 108-95-2,27073-41-2
phenol

: 192126-71-9
N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 120 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c2cc36719j

Reference yield:

: 118129-60-5
1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride

: 192126-71-9
N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1-methyl-pyrrolidin-2-one

2: potassium carbonate / 1-methyl-pyrrolidin-2-one / 3 h / 120 °C

With potassium carbonate; acetic acid; In 1-methyl-pyrrolidin-2-one;
DOI:10.1039/c3sc52344f

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 192126-71-9
N,N'-bis(cyclohexyl)-1,7-bis(phenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; iodine; sulfuric acid

2: acetic acid / 1-methyl-pyrrolidin-2-one

3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 3 h / 120 °C

With sulfuric acid; bromine; iodine; potassium carbonate; acetic acid; In 1-methyl-pyrrolidin-2-one;
DOI:10.1039/c3sc52344f